Electrolysis synthesis and characterization properties of nickel oxide nanoparticle

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Yanatra Budi Pramana, Yunia Dwie Nurcahyanie, Muhamad Abdul Jumali, Rhenny Ratnawati, Sugito

2018 Journal of Telecommunication, Electronic and Computer Engineering Vol. 10 Issue 2-3 Article Cited by 0 Quartile

Abstract

Synthesis nickel oxide nanoparticles based on electrolysis method at high voltage (55 V), with concentration natrium citrate optional condition at 0.3 M. The nickel oxide nanoparticles sample were characterized using, X-Ray Diffraction (XRD), Fourier Transform Infrared spectrometer (FTIR), Thermo Gravimetric Analysis (TGA), Scanning Electron Microscopy (SEM) and Transmission Electron Microscopy (TEM). XRD result show diffractogram from the product have the same lattice with standard ICDD, Thermogram shows at a temperature above 400°C already formed nickel oxide nanoparticles. Spherical nanoparticles were obtained by this method. © 2018 Universiti Teknikal Malaysia Melaka. All rights reserved.

Affiliations

Industrial Engineering Dept., Faculty of Engineering, University of PGRI Adi Buana, Surabaya, Indonesia; Environmental Engineering Dept., Faculty of Engineering, University of PGRI Adi Buana, Surabaya, Indonesia

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